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Characterization of Brown–Black and Blue Pigments in Glazed Pottery Fragments from Castel Fiorentino (Foggia, Italy) by Raman Microscopy, X-Ray Powder Diffractometry and X-Ray Photoelectron Spectroscopy

✍ Scribed by Robin J. H. Clark; Lucia Curri; Geoffrey S. Henshaw; Caterina Laganara


Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
260 KB
Volume
28
Category
Article
ISSN
0377-0486

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✦ Synopsis


Fragments from the archaeological site of Castel Fiorentino (Foggia, Italy) were analysed by Raman microscopy x-ray powder di †ractometry and x-ray photoelectron spectroscopy to determine the pigments used in the decoration of this medieval (13-14th century) pottery. Lapis lazuli was identiÐed as the blue pigment and such decoration was established as a characteristic of this pottery class. The brown-black pigment was identiÐed as a manganese oxide, probably

The qualitative composition of the glaze was also shown to include tin(IV) oxide MnO 2 . (cassiterite) and lead-containing oxides, along with other oxides.