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Characterization of acrylic bone cement using dynamic mechanical analysis

✍ Scribed by Yang, Jen-Ming ;Li, Hui-Min ;Yang, Ming-Chien ;Shih, Chun-Hsiung

Publisher: John Wiley and Sons
Year: 1999
Tongue: English
Weight: 203 KB
Volume: 48
Category: Article
ISSN: 0021-9304
DOI: 10.1002/(sici)1097-4636(1999)48:1<52::aid-jbm10>3.0.co;2-z

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✦ Synopsis

Dynamic mechanical analysis (DMA) was used to characterize the properties of acrylic bone cement with the addition of tricalcium phosphate (TCP), hydroxyethyl methacrylate (HEMA), and ethylene glycol dimethacrylate (EGDMA). The glass transition temperature of acrylic bone cement is ú100ЊC; the cement has a flat modulus response near human body temperature. The height of the damping peak decreases and becomes broader with increasing TCP content. Thus, TCP is incompatibile with acrylic bone cement. When the frequency is changed from high to low, the damping peak shifts to low temperature. The shift in damping peak with frequency indicates that this relaxation is time-dependent. When acrylic bone cement contains TCP with HEMA and EGDMA, the incompatibility between acrylic bone cement and TCP can be ameliorated.

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