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Characterization and monitoring of amitraz degradation products in honey

✍ Scribed by Jiméanez, Juan Joséa ;Bernal, Joséa Luis ;Del Nozal, María Jesús ;Toribio, Laura ;Atienza, Julián

Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
387 KB
Volume
20
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

Capillary gas chromatography in combination with atomic emission and electron impact‐chemical ionizaion mass spectrometry detectors have been used to detect amitraz degradation products in honey storage, characterize their structure, and evaluate their occurrence over a 100 day peroid. To this end, honey samples were extracted with an 8:2 v/v n‐hexane/acetone mixture. Amitraz was found to be rapidly decomposed into five related compounds, of which N‐(2,4‐dimethylphenyl)formamide was the most abundant and persistent.

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