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CC Coupling by Thermolysis of Alkynyl Phosphonium Borates

✍ Scribed by Xiaoxi Zhao; Prof. Dr. Thomas M. Gilbert; Prof. Dr. Douglas W. Stephan

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
277 KB
Volume
16
Category
Article
ISSN
0947-6539

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in ( 2) is probably bonded symmetrically to the two PO oxygen atoms as in the platinum complexes Pt[(PR20)2H]2 Reaction of (2) with HBF4 leads to (3), a complex containing the bis(dimethy1phosphito)difluoroborate ion hitherto unknown in the free state. Compound (2) reacts with NH3 to give the ammoni