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C−C and C−N Coupling Reactions of an Imidotitanium Complex with Isocyanides

✍ Scribed by Bashall, Allan; Collier, Philip E.; Gade, Lutz H.; McPartlin, Mary; Mountford, Philip; Pugh, Stephen M.; Radojevic, Sanja; Schubart, Martin; Scowen, Ian J.; Trösch, Dominique J. M.

Book ID
119941512
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
183 KB
Volume
19
Category
Article
ISSN
0276-7333

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Sulfene complexes [CpRu(PRЈ 3 ) 2 (RHC=SO 2 )]PF 6 (2aϪd) are obtained from the corresponding sulfur dioxide complexes 1aϪc and diazomethane or -ethane. Reaction of [CpRu(dppm)(SO 2 )]Cl (1d) and phenyldiazomethane gives the chlorobenzylsulfinato complex [CpRu(dppm)(SO 2 -CHPhCl)] (3). Alternatively