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Catalytic hypervalent iodine oxidation of alcohols to the corresponding carbonyl compounds using N -hydroxyphthalimide (NHPI) and m -chloroperbenzoic acid

✍ Scribed by Zhu, Chenjie; Ji, Lei; Zhang, Qian; Wei, Yunyang

Book ID: 118134049
Publisher: NRC Research Press
Year: 2010
Tongue: French
Weight: 337 KB
Volume: 88
Category: Article
ISSN: 0008-4042
DOI: 10.1139/v10-007

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✦ Synopsis

An efficient, facile, and mild oxidation of alcohols to the corresponding carbonyl compounds with m-chloroperbenzoic acid (mCPBA) and N-hydroxyphthalimide (NHPI) in the presence of a catalytic amount of iodobenzene was reported. The oxidation proceeded in mixed solvent at room temperature to afford carbonyl compounds in excellent yields. A possible mechanism for the oxidation was proposed.

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