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Catalytic hydrogenolysis as an alternative to the wolff-kishner or clemmensen reduction methods for azabicyclic ketones

✍ Scribed by Louis P. Reiff; Herbert S. Aaron


Book ID
104223963
Publisher
Elsevier Science
Year
1967
Tongue
French
Weight
161 KB
Volume
8
Category
Article
ISSN
0040-4039

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✦ Synopsis


Although hydrogenolysis of conjugated (i.e., allylic or bentylic) alcohols or ketones is a well known reaction (l), the hydrogenolysis of the unconjugated carbonyl group '(e.g., I -c II) is not a recognized synthetic procedure (2). We wish to report some results, summarized in the Table, which suggest that hydrogenolysis over platinum in acid may be a useful general