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Catalytic decomposition of 5-diazo-2,2-dimethyl-1,3-dioxane-4,6-dione and its analogs

✍ Scribed by V. V. Shevchenko; A. A. Shakhmin; V. A. Nikolaev

Book ID
111464176
Publisher
SP MAIK Nauka/Interperiodica
Year
2006
Tongue
English
Weight
436 KB
Volume
42
Category
Article
ISSN
1070-4280

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5-(Amino­methyl­ene)-2,2-dimethyl-1,3-dioxane-4,6-dione
✍ da Silva, Luiz Everson ;Joussef, Antonio Carlos ;Silva, Luciano Luiz ;Foro, Sabi 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 248 KB

In the title compound C 7 H 9 NO 4 , the 1,3-dioxane-4,6-dione ring exhibits an envelope conformation. Intermolecular hydrogen bonds connect the molecules into chains. One intramolecular N-HÁ Á ÁO hydrogen bond to a carbonyl O atom is also observed, forming a six-membered ring.

5-(Anilinomethyl­ene)-2,2-dimethyl-1,3-d
5-(Anilinomethyl­ene)-2,2-dimethyl-1,3-dioxane-4,6-dione
✍ Vencato, Ivo ;Cunha, Silvio ;Ferrari, Jailton ;Sabino, Jose R. 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 146 KB

Single-crystal X-ray study T = 297 K Mean (C-C) = 0.004 A Disorder in main residue R factor = 0.076 wR factor = 0.204 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.