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Catalytic and Solvophobic Promotion of High Pressure Addition Reactions

✍ Scribed by Gerard Jenner

Publisher
John Wiley and Sons
Year
2003
Weight
50 KB
Volume
34
Category
Article
ISSN
0931-7597

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3-Methylsulfanylfuran and 3-phenylsulfanylfuran were found to undergo facile, regioselective and stereoselective Diels-Alder (DA) cycloaddition to a variety of cycloalkenones under high pressure to give the corresponding ringannulated 7-oxabicyclo[2.2.

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separated in accordance with the procedure of Ross et al. The aqueous residues after removal of ethereal products were made alkaline and then extracted with ether, washed with water and dried. Removal of solvent afforded amines, meltingat 114Β°-1150C(Lit.8m.p. 115Β°-1180C) andmixedmelting points of th