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Catalysis-Based Total Synthesis of Latrunculin B

✍ Scribed by Alois Fürstner; Dominic De Souza; Liliana Parra-Rapado; Jon T. Jensen

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
119 KB
Volume
42
Category
Article
ISSN
0044-8249

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Scheme 1. Retrosynthetic analysis of latrunculin B. Scheme 2. Synthesis of two building blocks by iron-catalyzed crosscoupling reactions: a) KHMDS, PhN(Tf) 2 , THF, À 78 8C, 61 %; b) [Fe(acac) 3 ] (10 mol %), THF, À 30 8C, 97 %; c) aqueous NaOH, MeOH, 92 %; d) CDI, THF, 71 %; e) NaH, PMBBr, THF, 77

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