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Carbonate-Assisted Hydrothermal Synthesis of Nanoporous CuO Microstructures and Their Application in Catalysis

✍ Scribed by Min Zhou; Yan'an Gao; Baoxiang Wang; Zbigniew Rozynek; Jon Otto Fossum

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
863 KB
Volume
2010
Category
Article
ISSN
1434-1948

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✦ Synopsis

We have demonstrated a facile carbonate-assisted hydrothermal route for synthesis of well-defined nanoporous copper oxide microstructures with high surface area. The nanoporous CuO microstructures were synthesised by adding sodium hydrogen carbonate (NaHCO 3 ) to an aqueous solution of copper chloride (CuCl 2 ) in the presence of poly(vinylpyrrolidone) (PVP) at 300 °C. The introduction of NaHCO 3 is critical for the successful synthesis of porous nanoarchitectures owing to the formation of carbon dioxide (CO 2 ) gas dur-

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