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Carbon-13 T1 measurements of medium and large ring cycloalkanes and a catenane

✍ Scribed by H Fritz; P Hug; H Sauter; E Logemann


Book ID
103186804
Publisher
Elsevier Science
Year
1976
Weight
213 KB
Volume
21
Category
Article
ISSN
0022-2364

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Synthesis of Medium and Large Ring Compo
✍ Kraft, Philip ;Tochtermann, Werner πŸ“‚ Article πŸ“… 1994 πŸ› John Wiley and Sons 🌐 English βš– 377 KB

## Abstract The title compound (+)‐3 was synthesized in four steps by ring enlargement of cyclodecanone (6) with the chiral building block 5. The protected hydroxy halide 5, easily prepared from commercially available (2__S__)‐(+)‐methyl 3‐hydroxy‐2‐methylpropanoate (4), was introduced by HMPA‐medi