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Carbon-13 solid-state NMR of soil organic matter - using the technique effectively

✍ Scribed by Preston, Caroline M

Book ID
118280210
Publisher
Agricultural Institute of Canada
Year
2001
Tongue
English
Weight
287 KB
Volume
81
Category
Article
ISSN
0008-4271

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πŸ“œ SIMILAR VOLUMES

Background Signal in Solid State 13C NMR
Background Signal in Solid State 13C NMR Spectra of Soil Organic Matter (SOM)β€”Quantification and Minimization
✍ Ronald J. Smernik; J.Malcolm Oades πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 English βš– 112 KB

13 C background signal, obtained for an empty rotor, was shown by spin counting experiments to be equivalent to 1 mg of observable carbon for cross-polarization (CP) spectra and 69 mg of observable C for Bloch decay (BD) spectra. The BD background was mainly due to Kel-F in the stator, with minimal