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Carbon-13 nuclear magnetic resonance spectra. XVI—lanthanide induced signal shifts of diastereotopic 13C nuclei as a probe for a conformational equilibrium

✍ Scribed by Helmut Duddeck; Volker Wiskamp


Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
161 KB
Volume
15
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

The ^13^C NMR signals of the two methyl groups in 4‐hydroxy‐1‐isopropyl‐2‐oxaadamantane are anisochronous in the presence of Yb(fod)~3~. This is interpreted in terms of the different populations of three rotational conformers.