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Carbon-13 NMR spectra of all-trans-N-retinylidene-n-butylamine as an analogue of the Schiff's base linkage-compound in visual pigment

✍ Scribed by Yasuo Tokitô; Yoshio Inoue; Riichirô Chûjô; Yasuhiro Miyoshi


Publisher
John Wiley and Sons
Year
1975
Tongue
English
Weight
277 KB
Volume
7
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

Carbon‐13 NMR spectra have been obtained for all‐transN‐retinylidene‐n‐butylamine as an analogue of the Schiff's base linkage compound in visual pigment. The chemical shift changes on going from all‐trans‐retinal~1~ to all‐transN‐retinylidene‐n‐butylamine are observed. These changes indicate the collapse of the bond alternation in conjugated polyene carbons, whereas N‐protonation in all‐transN‐retinylidene‐n‐butylamine does not affect the bond alternation.