956, Buenos Aires (1 113), Argentina I3C CP/MAS NMR spectra of nitrogen-containing compounds often show complex signals when recorded at low field strengths. This effect is due to the 13C, '"N residual dipolar coupling which is not averaged to zero by magic-angle spinning. Solidstate 13C NMR spectra
Carbon-13 NMR of solid phenylazo-2-naphthols: Tautomerism and (13C, 14N) residual dipolar coupling
β Scribed by Robin K. Harris; Paul Jonsen; Kenneth J. Packer; Colin D. Campbell
- Publisher
- John Wiley and Sons
- Year
- 1986
- Tongue
- English
- Weight
- 895 KB
- Volume
- 24
- Category
- Article
- ISSN
- 0749-1581
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This work explores the utility of simple rotary resonance experiments for the determination of the magnitude and orientation of 13 C chemical shift tensors relative to one or more 13 C-14 N internuclear axes from 13 C magic-angle-spinning NMR experiments. The experiment relies on simultaneous recoup
## Abstract Solidβstate nuclear magnetic resonance (SSNMR) is a powerful technique for the structural analysis of amyloid fibrils. With suitable isotope labelling patterns, SSNMR can provide constraints on the secondary structure, alignment and registration of Ξ²βstrands within amyloid fibrils and i