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Carbon-13 chemical shielding tensors in acetic acid

✍ Scribed by J. van Dongen Torman; W.S. Veeman; E. De Boer

Publisher
Elsevier Science
Year
1977
Tongue
English
Weight
384 KB
Volume
24
Category
Article
ISSN
0301-0104

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πŸ“œ SIMILAR VOLUMES

Carbon-13 shielding tensors for metal ac
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## Abstract Carbon‐13 shielding tensor data for eight metal acetates, obtained by analysis of spinning sideband manifolds of slowspinning CP/MAS spectra, are presented and discussed.

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The principal elements of 13C chemical shift tensors in some dicarboxylic acids were determined from powder samples by two methods: (i) from the theoretical fit of the experimental data and (ii) from the sideband intensities of the CP-MAS spectra using the graphical procedure of Herzfeld and Berger.

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✍ K. Takegoshi; C.A. McDowell πŸ“‚ Article πŸ“… 1986 πŸ› Elsevier Science 🌐 English βš– 527 KB

The orientations of the principal axes of the 13C chemical shielding tensor of the double-bonded C5 carbon nucleus in smgle crystals of 1,1,2,2-tetraacetylethane are essentially identical with those of an aromatIc carbon nucleus. That observation and the similarities between the tensors of the carbo