✦ LIBER ✦

Capillary supercritical fluid chromatography of limonoids

✍ Scribed by Raynor, Mark W. ;Roberts, Sianne L. ;Mulholland, Dulcie A.

Publisher: John Wiley and Sons
Year: 1993
Tongue: English
Weight: 400 KB
Volume: 16
Category: Article
ISSN: 0935-6304
DOI: 10.1002/jhrc.1240160805

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

Capillary supercritical fluid chromatography (SFC) with carbon dioxide as the mobile phase has been used to separate a mixture of limonoid standards. Chromatographic conditions were optimized to enable analysis of plant extracts. The seed of Aphanamixis polystacha (Meliaceae) and the stem bark of Harpephyllum caffrum (Anacardiaceae) were extracted with hexane and the extracts were analyzed by SFC to demonstrate the potential of the technique as a screening tool. SFC analysis indicated the presence of limonoids in the hexane extract of the bark of Entandrophragma delevoyii (Meliaceae). One limonoid and two protolimonoids isolated from the extract were separated by SFC.

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