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Capillary GC on 50 micrometer I.D. Columns coated with thick films. Theory and selected practical results

✍ Scribed by Steenackers, Dirk ;Sandra, Pat


Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
554 KB
Volume
18
Category
Article
ISSN
0935-6304

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✦ Synopsis


Abstract

The chromatographic performance of 50 μm internal diameter (i.d.) fused silica columns coated with up to 2 μm films of immobilized SE‐54 (methyl phenyl (5%) silicone) is evaluated under gas chromatographic conditions. The influence of pressure drop on the plate height is discussed. In comparison to thick film 250–530 μm i.d. columns, much higher efficiencies and faster analyses are obtained. Practical examples, performed on a standard GC instrument, illustrate the features of thick film 50 μm i.d. columns.