## Abstract Epoxidation of 3‐phenoxycyclohexene **5** with __m__‐chloro‐perbenzoic acid gave **6** and **7** in a ratio of 9:1. These two epoxides were heated with a series of amines to give the aminophenoxycyclohexanol derivatives **1** and **2** respectively; in all cases the reaction was regio‐
Capillary GC analysis of the stereoisomers of 2-methylperhydroisoquinolin-6-one and 2-decalone
✍ Scribed by Harden, Raymond C. ;Rackham, David M.
- Publisher
- John Wiley and Sons
- Year
- 1992
- Tongue
- English
- Weight
- 177 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0935-6304
No coin nor oath required. For personal study only.
✦ Synopsis
Following this simple work-up procedure, the values measured for the specific rotation [al;,,. (in methanol) of the (-) and (+)
enantiomers were -95.4" and +93.9", respectively.
Industries, CA, USA.
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