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Capillary electrochromatography with monolithic silica columns: III. Preparation of hydrophilic silica monoliths having surface-bound cyano groups: chromatographic characterization and application to the separation of carbohydrates, nucleosides, nucleic acid bases and other neutral polar species

✍ Scribed by Darin Allen; Ziad El Rassi

Book ID: 108092009
Publisher: Elsevier Science
Year: 2004
Tongue: English
Weight: 427 KB
Volume: 1029
Category: Article
ISSN: 1873-3778
DOI: 10.1016/j.chroma.2003.12.015

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## Abstract Monolithic silica columns with surface‐bound octadecyl (C18) moieties have been prepared by a sol‐gel process in 100 μm ID fused‐silica capillaries for reversed‐phase capillary electrochromatography of neutral and charged species. The reaction conditions for the preparation of the C18‐