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Can a gradient crystal compete with a mosaic crystal as a monochromator in neutron- or X-ray diffraction?

✍ Scribed by K.-D. Liss; A. Magerl

Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
672 KB
Volume
338
Category
Article
ISSN
0168-9002

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A simple molecule with a complex crystal structure: interplay of 31P solid-state NMR spectroscopy and single-crystal x-ray diffraction in the structure determination of a ruthenium diphosphine diamine complex
✍ Klaus Eichele; Christiane Nachtigal; Susanne Jung; Hermann A. Mayer; Ekkehard Li 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 174 KB

## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should