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Calycanthine monohydrate

✍ Scribed by Vencato, Ivo ;Lariucci, Carlito ;Oliveira, Cecilia M. A. de ;Kato, Lucilia ;Nascimento, Claudia A. do

Book ID: 104482018
Publisher: International Union of Crystallography
Year: 2004
Tongue: English
Weight: 233 KB
Volume: 60
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s160053680401178x

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✦ Synopsis

The title compound [systematic name: 21,24-dimethyl-3,12,21,24-tetraazahexacyclo[9.7.3.3 2,10 .0 1,10 .0 4,9 .0 13,18 ]tetracosa-4,6,8,13(18),14,16-hexaene monohydrate], C 22 H 28 N 4 Á-H 2 O, crystallizes in space group P2 1 2 1 2 1 with Z = 4 and exhibits approximate C 2 symmetry. Intermolecular hydrogen bonds [OÐHÁ Á ÁN = 2.872 (3) and NÐHÁ Á ÁO = 3.062 (4) A Ê ] form chains along the direction [010].

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