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Calorimetric diagnostic of convergence of solute particles during a heating of frozen aqueous solutions

โœ Scribed by A.M. Kaplan; O.I. Mikhalev; O.I. Kovalev; V.I. Trofimov

Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
170 KB
Volume
92
Category
Article
ISSN
0040-6031

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Proton MAS NMR of a protein in a frozen
Proton MAS NMR of a protein in a frozen aqueous solution
โœ F. Volke; A. Pampel; M. Haensler; G. Ullmann ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 252 KB

~H MAS NMR spectra of et-chymotrypsin in aqueous solution and in ice are presented. The MAS technique allows one to resolve mobile protein polypeptide side chains, even at subzero temperature (248 K). Determination of the amount of non-freezing water at the protein-ice interface using MAS NMR is of