Calibration and testing of an isoperibolic micro-combustion calorimeter developed to measure the enthalpy of combustion of organic compounds containing C, H, O and N

A micro-combustion calorimeter suitable

A micro-combustion calorimeter suitable for samples of mass 10 mg to 50 mg. Application to solid compounds of C, H, and O, and of C, H, O, and N

✍ Hermı&#x0301;nio P. Diogo; Manuel E. Minas da Piedade 📂 Article 📅 1995 🏛 Elsevier Science 🌐 English ⚖ 524 KB

A micro-combustion calorimeter suitable for samples of mass about 10 mg to 50 mg is described. Calibration with benzoic acid led to the energy equivalent o°= (1809.82 2 0.28) J•K -1 . The calorimeter was tested by determining the standard molar enthalpies of formation at the temperature 298.15 K of