𝔖 Bobbio Scriptorium
✦   LIBER   ✦

CaB6 single crystals grown under high pressure and hightemperature

✍ Scribed by Shengwei Xin; Xianyue Han; Shaocun Liu; Zhongyuan Liu; Bo Xu; Yongjun Tian; Dongli Yu

Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
899 KB
Volume
313
Category
Article
ISSN
0022-0248

No coin nor oath required. For personal study only.

✦ Synopsis

Millimeter-sized single crystals of CaB 6 are obtained by the reaction of B and Ca under 1 GPa and 950-1150 1C. The structure, chemical composition, and morphologies of the crystals are characterized by X-ray diffraction and field emission scanning electron microscopy with energy dispersion spectrometry. Investigation of the growth mechanism of CaB 6 single crystals indicates that the growth temperature affects the shape of the crystals. Electric resistivity dependence tests of temperatures from 2 to 300 K show that CaB 6 single crystals are conductive materials with semi-metallic behaviors.

πŸ“œ SIMILAR VOLUMES

Transport properties of single crystals
Transport properties of single crystals with high Pr-site filling fraction grown under high pressure
✍ Kenya Tanaka; Takahiro Namiki; Takashi Saito; Sho Tatsuoka; Atsushi Imamura; Kei πŸ“‚ Article πŸ“… 2009 πŸ› Elsevier Science 🌐 English βš– 321 KB

We have succeeded in growing Pr x Os 4 Sb 12 single crystals under $4 GPa with high Pr-site filling fraction x. The electrical resistance measurements clearly show that the superconducting (SC) transition is sharper and the onset temperatures is lower in the single crystal samples grown under high p

Real carbon source of diamond single cry
Real carbon source of diamond single crystals grown in the Fe–Ni–C system under high temperature and high pressure
✍ He-sheng Li; Mu-sen Li; Jian-jun Cui πŸ“‚ Article πŸ“… 2010 πŸ› Elsevier Science 🌐 English βš– 39 KB

Carbon microspheres (CMSs) were synthesized by chemical vapor deposition in an Ar atmosphere using deoiled asphalt as carbon source. KMnO 4 aqueous solutions with different concentrations were used to oxidize the CMSs to form MnO 2 -coated CMSs (MnO 2 /CMS composites) and H 2 C 2 O 4 solution was us