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Bromomethylation; Preparation of 2,6-Bis-(bromomethyl)-4-alkyl Phenols

✍ Scribed by Bright, Willard M.; Cammarata, Peter

Book ID
126285543
Publisher
American Chemical Society
Year
1952
Tongue
English
Weight
161 KB
Volume
74
Category
Article
ISSN
0002-7863

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## Abstract Under basic conditions 2,6‐bis(bromomethyl)‐4‐pyrone **8** reacts with tetraethylene glycol to yield the unexpected macrocycle **9**, which is related to the antibiotic Kjellmanianone **10**. We propose that this ring transformation proceeds __via__ the cyclopropyl intermediate **d** (S