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Bonding in the first-row transition-metal monocarbonyl molecules

✍ Scribed by Bach, S. B. H.; Taylor, C. A.; Van Zee, R. J.; Vala, M. T.; Weltner, W.

Book ID
126154189
Publisher
American Chemical Society
Year
1986
Tongue
English
Weight
284 KB
Volume
108
Category
Article
ISSN
0002-7863

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## Abstract Lithiated 4‐methyl‐2‐[(trimethylsilyl)amino]pyridine (Ap^TMS^H) undergoes a salt metathesis reaction with [ScCl~3~(thf)~3~] and FeCl~3~, at low temperature in thf, to yield the homoleptic complexes [Sc(Ap^TMS^)~3~] (1) and [Fe(Ap^TMS^)~3~] (2). An analogous reaction with MnCl~2~, CoCl~2