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Bis[tris(1,3-diaminopropane)manganese(II)] octasulfidotetraantimonate(III) dihydrate

✍ Scribed by Engelke, Lars ;Bensch, Wolfgang

Publisher: International Union of Crystallography
Year: 2003
Tongue: English
Weight: 158 KB
Volume: 59
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536803011036

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✦ Synopsis

Yellow crystals of [Mn(pn) 3 ] 2 [Sb 4 S 8 ]Á2H 2 O (pn = 1,2-diaminopropane) were synthesized under solvothermal conditions by reacting elemental Mn, Sb and S in an aqueous solution of 1,2diaminopropane. The structure is composed of cyclic [Sb 4 S 8 ] 4À anions and octahedral [Mn(pn) 3 ] 2+ cations, both stacked in a rod-like manner along the a axis. The anion sits on a centre of symmetry. Between the anions and the cations there is an extended hydrogen-bonding network.

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✦ Synopsis

Bis[tris(1,3-diaminopropane)manganese(II)] octasulfidotetraantimonate(III) dihydrate