Bis(triphenylsilyl)phenylarsenite, PhAs(OSiPh3)2
✍ Scribed by Ferguson, George ;O'Leary, Brian J. ;Spalding, Trevor R.
- Book ID
- 104481327
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 196 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.002 A Ê Disorder in main residue R factor = 0.059 wR factor = 0.192 Data-to-parameter ratio = 21.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 130 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.046 wR factor = 0.126 Data-to-parameter ratio = 11.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 113 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.133 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
ÁC 48 H 60 BF 16 Si 4 À , consists of discrete cations and anions. There are two ions of each kind in the asymmetric unit.
The title compound, [Ru 3 ( 3 -NC 6 H 4 Br) 2 (CO) 9 ], is a V-shaped triruthenium cluster, each side of the V being face-capped by a 4-bromophenylimide ligand. Each Ru atom is also ligated by three terminal carbonyl ligands. There are two molecules in the asymmetric unit with minor conformational d