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Bis(trifluorophosphine)diborane(4)

✍ Scribed by Deever, William R.; Lory, Earl R.; Ritter, David M.

Book ID
126057016
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
678 KB
Volume
8
Category
Article
ISSN
0020-1669

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πŸ“œ SIMILAR VOLUMES

Diborane(4)-bis(trifluorophosphine) addu
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## ray structures Indenyllithium reacts with dichlorobis(dimethylamino)diborane(4) with formation of bis(dimethylamino)bis(1-indenyl)diborane(4) which rearranges on heating to the isomer bis(dimethylamino)bis(3-indenyl)diborane(4). The "mixed" bis(dimethylamino)(1-indenyl)(3-indenyl)diborane( 4) i

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gives yellow needles, m.p. 322--324 "C (from n-butanol), Amax (in chloroform): 242 my (log E = 4.59), 275 (4.47), 31 5 (shoulder), 368 (shoulder); broad band with indistinct structure at 405 my (log E = 4.10). It dissolves in conc. HlS04 to give a carmine-red solution, A , , , , (in H2SO4): 251 mp (