Bis(tetraethylammonium) bis(dimethylammonium) dihydrogendecavanadate(V)
✍ Scribed by Chen, Lian ;Yue, Cheng-Yang ;Yuan, Da-Qiang ;Jiang, Fei-Long ;Hong, Mao-Chun
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 309 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, (C~2~H~8~N)~2~(C~8~H~20~N)~2~[H~2~V~10~O~28~], contains two crystallographically independent centrosymmetric polyvanadate clusters, each with a composition [V~10~O~28~H~2~]^4−^, with the H atoms attached to μ~2~-O atoms. A variety of O—H...O and N—H...O hydrogen bonds generate a two-dimensional network.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 295 K Mean '(N±C) = 0.003 A Ê R factor = 0.031 wR factor = 0.078 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.050 wR factor = 0.124 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.