Single-crystal X-ray study T = 160 K Mean '(C±C) = 0.002 A Ê R factor = 0.041 wR factor = 0.116 Data-to-parameter ratio = 21.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Bis(dimethylammonium) 1,4-phenylenediacrylate
✍ Scribed by Wheeler, Kraig A. ;Deschamps, Jeffrey R.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 230 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, 2 C 2 H 8 N + ÁC 12 H 8 O 4 2À , crystallizes as a salt in space group P2 1 /n, the anion being located on an inversion center. The dimethylammonium cations link neighboring carboxylate anions via two N + ÐHÁ Á ÁO hydrogen bonds [HÁ Á ÁO = 1.72 (3) and 1.84 (3) A Ê , NÁ Á ÁO = 2.671 (2) and 2.726 (2) A Ê , and NÐHÁ Á ÁO = 178 (3) and 173 (2) ] resulting in molecular ribbons.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.060 wR factor = 0.171 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.002 A Ê R factor = 0.043 wR factor = 0.128 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 24 H 18 , possesses a twofold rotation axis, which bisects the 1,2-dimethylbenzene ring. In the crystal structure, all three benzene rings are essentially coplanar, the angle between the central and terminal rings being 3.8 (1) .