๐”– Bobbio Scriptorium
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Bis(dialkoxy phosphato) chelates of nickel(II) as acceptors

โœ Scribed by Ram Chand Paul; V.P. Kapila; R.S. Battu; S.K. Sharma


Book ID
103105781
Publisher
Elsevier Science
Year
1977
Weight
138 KB
Volume
13
Category
Article
ISSN
0020-1650

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131 Experimenfal Procedure for 2 and 4d4b (cf. [12a]): terf-Butyllithium (15-18 mmol in pentane/hexane) is added dropwise to a solution of 1ethoxyethene (7.0 mmol) or of I-ethoxypropene (E/Z=28 :72) in 10 mL THF (or 5.0 mL pentane with 7.0 mmol TMEDA) under an inert gas atmosphere at -74"C, the mixt