Bis[2-(cycloheptyliminomethyl)pyridine-κ2N,N′]silver(I) tetraphenylborate
✍ Scribed by Massa, Werner ;Dehghanpour, Saeed ;Tashakori, Gilda ;Aoki, Katsuyuki
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 966 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
V = 4200.03 (16) A ˚3 Z = 4 Mo K radiation = 0.52 mm À1 T = 100 (2) K 0.50 Â 0.38 Â 0.24 mm Data collection Stoe IPDSII diffractometer Absorption correction: multi-scan (Blessing, 1995) T min = 0.781, T max = 0.886 32871 measured reflections 11472 independent reflections 10372 reflections with I > 2(I) R int = 0.017 Refinement R[F 2 > 2(F 2 )] = 0.030 wR(F 2
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.011 A Ê Disorder in solvent or counterion R factor = 0.055 wR factor = 0.174 Data-to-parameter ratio = 11.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.007 A Ê R factor = 0.037 wR factor = 0.098 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.045 wR factor = 0.133 Data-to-parameter ratio = 20.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.