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Biomimetic Synthesis of trans,syn,trans-Fused Polycyclic Ethers

โœ Scribed by Jason C. Valentine; Frank E. McDonald

Publisher
John Wiley and Sons
Year
2006
Weight
8 KB
Volume
37
Category
Article
ISSN
0931-7597

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The reaction products were fractionated in a 2-mpackedcolumn. (2a) + (2b) (z 1 :l), b.p. 74-74.5 'C,%O torr, n: = 1.4898. (2a) + (26) stillcontained 4 % of cis,cis-l,3-cyclooctadiene. This additional compound can be detected gas chromatographically only after hydrogenation. (3), b.p. 67 "CjlOO torr,