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Benzyl (1R*,3S*)-3,6-di­hydro-3-methyl-1λ4,2-thia­zine-2-carboxyl­ate 1-oxide

✍ Scribed by Hansen, Lars Kr. ;Bayer, Annette ;Gautun, Odd R.


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
170 KB
Volume
58
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.035 wR factor = 0.107 Data-to-parameter ratio = 10.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


📜 SIMILAR VOLUMES


(1R*,3R*,6S*)-3,6-Di­hydro-3,6-di­methyl
✍ Hansen, Lars Kr. ;Bayer, Annette ;Gautun, Odd R. 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 207 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.003 A Ê R factor = 0.038 wR factor = 0.117 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 12 H 15 NO 3 S 2 , is shown to be the exo isomer with a cis arrangement of the S O group and the methyl group in the thiazine ring.

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✍ Alam, Samina ;Hasan, Mashooda ;Saeed, Sadaf ;Fischer, Andreas ;Khan, Naeema 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 191 KB

The title compound, C 14 H 16 N 2 O 2 , was obtained from the reaction between S-tryptophan methyl ester hydrochloride and acetaldehyde. The molecule adopts a trans configuration, with the methyl and methoxycarbonyl groups located on opposite sides of the central tetrahydro--carboline unit. Bifurcat