Benzo[c]furans
✍ Scribed by P. G. Steel
- Publisher
- John Wiley and Sons
- Year
- 2003
- Weight
- 46 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0931-7597
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✦ Synopsis
Abstract
For Abstract see ChemInform Abstract in Full Text.
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## Abstract It is shown that heptaleno[1,2‐__c__]furans 1, which are available in two steps from heptalene‐4,5‐dicarboxylates by reduction and oxidative dehydrogenation of the corresponding vicinal dimethanols 2 with MnO~2~ or IBX (__Scheme 4__), react thermally in a __Diels–Alder__‐type [4+2] cycl
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê Disorder in main residue R factor = 0.036 wR factor = 0.092 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.