Benzimidazolium 2-chloro-4-nitrobenzoate
✍ Scribed by Ishida, Hiroyuki ;Fukunaga, Takeo ;Kashino, Setsuo
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 145 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Crystals of (I) were obtained by slow evaporation from an acetonitrile solution of benzimidazole and 2-chloro-4-nitrobenzoic acid in a molar ratio of 1:1.
📜 SIMILAR VOLUMES
In the title compound, C~5~H~6~N^+^·C~8~H~4~NO~6~ ^−^, N—H...O and O—H...O hydrogen bonds stabilize the crystal structure.
The title compound, C 13 H 9 ClOS, crystallizes in the orthorhombic system in the non-centrosymmetric space group P2 1 2 1 2 1 , with one molecule in the asymmetric unit. The repulsion between two Cl atoms of neighbouring molecules is minimized by a 2 1 screw arrangement of the asymmetric unit.