Synthesis of [8,9,10,11-13C4]leukotriene
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Mark J. Raftery; Simon J. Gaskell
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Article
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1991
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John Wiley and Sons
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French
β 273 KB
## Abstract A βone potβ reduction of ethyl [1,2β^13^C~2~]bromoacetate with diisobutylaluminium hydride in dichloromethane, followed by reaction with triphenylphosphine, then triethylamine, yields [1,2β^13^C~2~]formylmethylenetriphenylphosphorane. Consecutive Wittig reactions of [1,2β^13^C~2~] formy