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Beckmann rearrangement of cyclohexanone oxime to ε-caprolactam in microreactors

✍ Scribed by K. T. Zuidhof; M. H. J. M. de Croon; J. C. Schouten


Publisher
American Institute of Chemical Engineers
Year
2009
Tongue
English
Weight
589 KB
Volume
56
Category
Article
ISSN
0001-1541

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Formation of ε-caprolactam via catalytic
✍ Rex X Ren; Larisa D Zueva; Wei Ou 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 50 KB

Catalytic Beckmann rearrangement of cyclohexanone oxime in ionic liquids using P 2 O 5 or Eaton's reagent has been investigated. 1-n-Butyl-3-methylimidazolium hexafluorophosphate (bmiPF 6 ) gives superior results to those noted by earlier workers.