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Bausteine von Oligosacchariden, CI. Synthese von modifizierten Oligosacchariden derN-Glycoproteine zur Untersuchung der Substratspezifität derN-Acetylglucosaminyltransferase II des Trimming-Prozesses

✍ Scribed by Paulsen, Hans ;van Dorst, Johannes A. L. M. ;Reck, Folkert ;Meinjohanns, Ernst


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
979 KB
Volume
1992
Category
Article
ISSN
0947-3440

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✦ Synopsis


Building Units of Oligosaccharides, CI. — Synthesis of Modified Oligosaccharides of the N‐Glycoproteins Intended for Substrate Specificity Studies of N‐Acetylglucosaminyltransferase II of the Trimming Process

The trichloroacetimidate method was very successful for the synthesis of the tetrasaccharide octyl O‐(2‐acetamido‐2‐deoxy‐β‐D‐glucopyranosyl)‐(1→2)‐O‐(α‐D‐mannopyranosyl)‐(1→3)‐O‐[(α‐D‐mannopyranosyl)‐(1→6)]‐β‐D‐mannopyranoside (10). Further derivatives of the tetrasaccharide with a 4‐O‐methyl group 20 and with a 4‐deoxy group 28 were synthesized. The tetrasaccharides are intended for substrate specificity studies of the N‐acetylglucosaminyltransferase II of the trimming process in the biosynthesis of N‐glycoproteins.