𝔖 Bobbio Scriptorium
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Basic techniques of working on a solid phase: From ABC of the peptide synthesis to libraries of non-natural amino acids

✍ Scribed by E. V. Babaev; D. S. Ermolat’ev

Book ID
111460811
Publisher
Springer
Year
2010
Tongue
English
Weight
578 KB
Volume
80
Category
Article
ISSN
1070-3632

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The Barton radical decarboxylation on so
The Barton radical decarboxylation on solid phase. A versatile synthesis of peptides containing modified amino acids
✍ Maria Elena Attardi; Maurizio Taddei 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 99 KB

Barton esters were prepared starting from different carboxylic acids loaded on a Wang resin. Light induced fragmentation occurred giving a radical that reacted with CBrCl 3 to give the corresponding bromides, whereas conjugate addition to electron-poor alkenes proved to be less synthetically useful.