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Azetidinone antibiotics. 17. A rearrangement of penicillin sulfoxides to 3-methylenecephams via sulfinyl intermediates

✍ Scribed by Kukolja, Stjepan; Lammert, Steven R.; Gleissner, Michael R. B.; Ellis, Alvin I.

Book ID: 126937240
Publisher: American Chemical Society
Year: 1976
Tongue: English
Weight: 294 KB
Volume: 98
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00432a068

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Structural studies of intermediates in a

Structural studies of intermediates in antibiotic synthesis. I. The structures of penicillin sulfoxide rearrangement products: 2,3,5,6-tetrahydro-5-hydroxymethyl-6,6-dimethyl-1,3-dioxo-8-[(phenylacetyl)amino]-1H-imidazo[5,1-c][1,4]thiazine (I) , C17H19N3O4S, and 2,3,5,6-tetrahydro-6,6-dimethyl-1,3-dioxo-8-[(phenylacetyl)amino]-1H-imidazo[5,1-c][1,4]thiazine-5-carboxylic acid (II), C17H17N3O5S

✍ Haran, T. E. ;Nudelman, A. ;Shakked, Z. 📂 Article 📅 1983 🏛 International Union of Crystallography 🌐 English ⚖ 695 KB