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Avoiding oxidative degradation during sodium hydroxide/methyl iodide-mediated carbohydrate methylation in dimethyl sulfoxide

โœ Scribed by P.W. Needs; R.R. Selvendran

Book ID
107727219
Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
706 KB
Volume
245
Category
Article
ISSN
0008-6215

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Oxidation of oligoglycosyl alditols duri
Oxidation of oligoglycosyl alditols during methylation catalyzed by sodium hydroxide and iodomethane in methyl sulfoxide
โœ William S. York; Laura L. Kiefer; Peter Albersheim; Alan G. Darvill ๐Ÿ“‚ Article ๐Ÿ“… 1990 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 549 KB

Certain artifacts in the glycosyl-linkage analysis of oligoglycosyl alditols were shown to be caused by oxidation of the alditol moieties when 0-methylation was catalyzed by NaOH in Me,SO. The partially methylated alditol acetates derived from I-[\*HI-cellobiitol that was 0-methylated by this method