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Automated iodimetric determination of Cu+, Cu2+ and Cu3+ in the superconductor YBCO using a modified Gran plot technique

✍ Scribed by Jan Yperman; An De Backer; Ann Vos; Dirk Franco; Jules Mullens; Lucien C. Van Poucke

Book ID: 102982847
Publisher: Elsevier Science
Year: 1993
Tongue: English
Weight: 710 KB
Volume: 273
Category: Article
ISSN: 0003-2670
DOI: 10.1016/0003-2670(93)80197-s

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✦ Synopsis

An automated potentiometnc determmatlon of the oxygen content of the superconductor YBCO IS described The end-pomt of the titration IS found usmg a bnear Gran plot techmque Suitable equations are denved by which the number of tltratron pomts can be considerably reduced and the tltratlon can be stopped even before the eqmvalence pomt IS reached AutomatIon of the &etnc tltraaon can be performed m an easy manner Dunng the htratlon a good estimate of the eqmvalence volume can be calculated usmg only two tltratlon pomts

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