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Atom transfer radical polymerization of styrene with FeCl2/acetic acid as the catalyst system

โœ Scribed by Shenim Zhu; Deyue Yan; Guosheng Zhang

Book ID
106002864
Publisher
Springer
Year
2001
Tongue
English
Weight
135 KB
Volume
45
Category
Article
ISSN
0170-0839

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The atom transfer radical polymerization of styrene and methyl methacrylate with FeCl 2 /iminodiacetic acid as the catalyst system in bulk was successfully implemented at 70 and 110 ยฐC, respectively. The polymerization was controlled: the molecular weight of the resultant polymer was close to the ca

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Well-deยฎned polystyrenes with an a-C(CH 3 ) 2 (CN) and an v-chlorine atom end-groups, and narrow polydispersity (M n = 3000ยฑ4000 g mol ร€1 , M w /M n = 1.3ยฑ1.4) have been synthesized by a radical polymerization process using 2,2'-azobisisobutyronitrile(AIBN)/FeCl 3 /PPh 3 initiation system. When the