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Asymmetric syntheses of 2,5-dideoxy-2,5-imino-d-glucitol [(+)-DGDP] and 1,2,5-trideoxy-1-amino-2,5-imino-d-glucitol [(+)-ADGDP]

✍ Scribed by Davies, Stephen G.; Figuccia, Aude L.A.; Fletcher, Ai M.; Roberts, Paul M.; Thomson, James E.

Book ID
121741598
Publisher
Elsevier Science
Year
2014
Tongue
French
Weight
793 KB
Volume
70
Category
Article
ISSN
0040-4020

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## Abstract Fragmentation of methyl 3‐__O__‐benzyl‐6‐bromo‐2‐__O__‐(__tert__‐butyldimethylsilyl)‐6‐deoxy‐4‐__O__‐(4‐methoxybenzyl)‐α‐D‐mannopyranoside (2) and in situ reductive amination give (3__R__,4__S__,5__R__)‐6‐benzylamino‐4‐benzyloxy‐5‐(__tert__‐butyldimethylsilyloxy)‐3‐(4‐methoxybenzyloxy)h