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Asymmetric reduction of trifluoromethyl ketones containing a sulfur functionality by the alcohol dehydrogenase from Geotrichum

✍ Scribed by Kaoru Nakamura; Tomoko Matsuda; Makoto Shimizu; Tamotsu Fujisawa

Book ID: 108379022
Publisher: Elsevier Science
Year: 1998
Tongue: French
Weight: 573 KB
Volume: 54
Category: Article
ISSN: 0040-4020
DOI: 10.1016/s0040-4020(98)00439-6

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The o-position to the nitro group in 4-nitro-2-butanol or S-nitro-2-pentanol was acylated under DBU-catalysis after the hydroxy group was protected by a t-butyl dimethylsilyl group. The prcscnt method has been applied to the asymmetric stercosclcctive synthesis of a pheromone for Andrsna haemorrkoa