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Assignments of the 1H and 13C NMR spectra of 1,4-diazaphenanthrene (benzo[f]quinoxaline) derivatives

✍ Scribed by N. Defay; R. Nasielski-Hinkens; J. Nasielski

Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
398 KB
Volume
25
Category
Article
ISSN
0749-1581

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✦ Synopsis

The 'H and 13C NMR spectra of 1,4-diazaphenanthrene (benzo[f]quinoxaline) (1) and some of its derivatives have been fully assigned and most of the coupling constants have been measured. The compounds examined bear a piperidino or methoxy group at the 2or 3-position, or a chlorine atom at the 2-, 3-or 9-position. The spectra of the N-1-oxides of 1 and of 1,4,5,Wetraazaphenanthrene are also given. The syntheses are described.

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